WEKO3
アイテム
{"_buckets": {"deposit": "afae75bb-5559-4e7e-b26e-29a2bb93e5be"}, "_deposit": {"created_by": 13, "id": "5831", "owners": [13], "pid": {"revision_id": 0, "type": "depid", "value": "5831"}, "status": "published"}, "_oai": {"id": "oai:mie-u.repo.nii.ac.jp:00005831", "sets": ["462"]}, "author_link": ["13061", "13062", "13063", "13064"], "item_4_biblio_info_6": {"attribute_name": "書誌情報", "attribute_value_mlt": [{"bibliographicIssueDates": {"bibliographicIssueDate": "1997-12-01", "bibliographicIssueDateType": "Issued"}, "bibliographicPageEnd": "12", "bibliographicPageStart": "7", "bibliographicVolumeNumber": "19", "bibliographic_titles": [{"bibliographic_title": "三重大学生物資源学部紀要 = The bulletin of the Faculty of Bioresources, Mie University"}]}]}, "item_4_description_14": {"attribute_name": "フォーマット", "attribute_value_mlt": [{"subitem_description": "application/pdf", "subitem_description_type": "Other"}]}, "item_4_description_4": {"attribute_name": "抄録", "attribute_value_mlt": [{"subitem_description": "The contents of 4(5)-methylimidazole (4-MI) in hay and cereal straw treated with different levels of ammonia were investigated by combining ion-pair extraction with reversed-phase ion-pair liquid chromatography (HPLC) and together with photometry of the Ehrich diazo coupling products (λ= 498 nm). The diazo coupling colors corresponding to 4-MI contents in treated roughage were verified and subjected to a panel test, in order to develop a simple procedure for semi-quantitative determination capable to be used on farms. \nAmmonia-treated hay (3% NH3DM⁻¹) contained 14-81μg g⁻¹DM of 4-MI and the values were increased by increasing the levels of ammonia. 4-MI was not detected in ammonia-treated rice and wheat straw, irrespective of the ammonia levels. A significant correlation between the visible absorbance of 4-MI and HPLC values was found for the ammonia-treated ones. The diazo coupling colors at different4-MI contents were assigned as follows, according to the standard Munsell color table (4-MI ; 0μg g⁻¹DM=5Y8/14 ; 30μg g-1DM=5YR 7/14 ; 50μg g⁻¹DM=5YR 6.5/13 ; 80μg g⁻¹DM=2.5YR 6.5/12 ; 100μg g⁻¹DM=5.5/12 ; 150μg g⁻¹DM=9R 5.5/14 ; 200μg g⁻¹DM=6R 5.5/14). The panel test showed that the 4-MI contents in the ammonia-treated hay were estimated by four groups of None, 30-50, 80-100 and \u003e 100μg g⁻¹DM, according to the Munsell analysis.", "subitem_description_type": "Abstract"}, {"subitem_description": "アンモニア処理された粗飼料中に副生される4(5)-メチルイミダゾール量を,材料の種類(牧草 イネ藁,麦稈)やアンモニア濃度(0,1,2,3,4,6,9%)との関係を検討した。また,生産現場などで簡単に4(5)-メチルイミダゾール量を検出する方法として,ジアゾカップリング呈色皮応によるマンセル値と標準色彩表(色相・明度・彩度)が有効であるかどうかを,パネルテストで判定した。\n稲わらや麦稈からの4(5)-メチルイミダゾールは,アンモニア処理の濃度と関係なく,ほとんど検出されなかった。一方,牧乾草の場合には,アンモニア濃度3%処理区で14~81μgg⁻¹DM,6%処理区100~176μgg⁻¹DM,9%処理区127~190μgg⁻¹DMと,アンモニア濃度の増加に対応して4(5)-メチルイミダゾール生成量が増加した。\nマンセル値と標準色彩表に基づいたパネルテストによる4(5)-メチルイミダゾールの濃度判定結果は,その濃度が0μggDM⁻¹(ブランク),50μgg⁻¹DM,176μgg⁻¹DMにおいてそれぞれ100%,87.5%,96.0%ときわめて高かった。18.8%の正解率となった30μgg⁻¹DMサンプルはおもに50μgg⁻¹DMと,31.3%の正解率となった100μgg⁻¹DMサンプルは80μgg⁻¹DMと判定された。総じて,パネリストによる判定は正確なものであった。", "subitem_description_type": "Abstract"}]}, "item_4_publisher_30": {"attribute_name": "出版者", "attribute_value_mlt": [{"subitem_publisher": "三重大学生物資源学部"}]}, "item_4_source_id_7": {"attribute_name": "ISSN", "attribute_value_mlt": [{"subitem_source_identifier": "0915-0471", "subitem_source_identifier_type": "PISSN"}]}, "item_4_source_id_9": {"attribute_name": "書誌レコードID", "attribute_value_mlt": [{"subitem_source_identifier": "AN10073846", "subitem_source_identifier_type": "NCID"}]}, "item_4_subject_16": {"attribute_name": "日本十進分類法", "attribute_value_mlt": [{"subitem_subject": "643", "subitem_subject_scheme": "NDC"}]}, "item_4_text_18": {"attribute_name": "その他のタイトル", "attribute_value_mlt": [{"subitem_text_language": "en", "subitem_text_value": "Munsell color Analysis of 4(5)-Methylimidazole Produced in Ammonia-treated Forage Relation to a Simple Prediction of Hyperexcitability in Cattle fed These Types of Forage"}]}, "item_4_text_63": {"attribute_name": "ノート", "attribute_value_mlt": [{"subitem_text_value": "Agropedia提供データ"}]}, "item_4_text_65": {"attribute_name": "資源タイプ(三重大)", "attribute_value_mlt": [{"subitem_text_value": "Departmental Bulletin Paper / 紀要論文"}]}, "item_4_version_type_15": {"attribute_name": "著者版フラグ", "attribute_value_mlt": [{"subitem_version_resource": "http://purl.org/coar/version/c_970fb48d4fbd8a85", "subitem_version_type": "VoR"}]}, "item_creator": {"attribute_name": "著者", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "横江, 泰彦", "creatorNameLang": "ja"}, {"creatorName": "Yokoe, Yasuhiko", "creatorNameLang": "en"}], "nameIdentifiers": [{"nameIdentifier": "13061", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "後藤, 正和", "creatorNameLang": "ja"}, {"creatorName": "Goto, Masakazu", "creatorNameLang": "en"}], "nameIdentifiers": [{"nameIdentifier": "13062", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "西川, 司朗", "creatorNameLang": "ja"}, {"creatorName": "Nishikawa, Shiro", "creatorNameLang": "en"}], "nameIdentifiers": [{"nameIdentifier": "13063", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "萬田, 富治", "creatorNameLang": "ja"}, {"creatorName": "Manda, Tomiharu", "creatorNameLang": "en"}], "nameIdentifiers": [{"nameIdentifier": "13064", "nameIdentifierScheme": "WEKO"}]}]}, "item_files": {"attribute_name": "ファイル情報", "attribute_type": "file", "attribute_value_mlt": [{"accessrole": "open_date", "date": [{"dateType": "Available", "dateValue": "2017-02-18"}], "displaytype": "detail", "download_preview_message": "", "file_order": 0, "filename": "AN100738460001902.pdf", "filesize": [{"value": "383.9 kB"}], "format": "application/pdf", "future_date_message": "", "is_thumbnail": false, "licensetype": "license_note", "mimetype": "application/pdf", "size": 383900.0, "url": {"label": "AN100738460001902.pdf", "url": "https://mie-u.repo.nii.ac.jp/record/5831/files/AN100738460001902.pdf"}, "version_id": "8e6fee59-6f22-4acd-8f38-b97f5c3f4e6c"}]}, "item_keyword": {"attribute_name": "キーワード", "attribute_value_mlt": [{"subitem_subject": "ammonia treatment", "subitem_subject_scheme": "Other"}, {"subitem_subject": "cereal straw", "subitem_subject_scheme": "Other"}, {"subitem_subject": "diazo coupling colors", "subitem_subject_scheme": "Other"}, {"subitem_subject": "hay", "subitem_subject_scheme": "Other"}, {"subitem_subject": "4(5)-methylimidazole analysis", "subitem_subject_scheme": "Other"}]}, "item_language": {"attribute_name": "言語", "attribute_value_mlt": [{"subitem_language": "jpn"}]}, "item_resource_type": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"resourcetype": "departmental bulletin paper", "resourceuri": "http://purl.org/coar/resource_type/c_6501"}]}, "item_title": "アンモニア処理草中の4(5)-メチルイミダゾールのマンセル分析とそのhyperexcitability発症の簡易予見への活用", "item_titles": {"attribute_name": "タイトル", "attribute_value_mlt": [{"subitem_title": "アンモニア処理草中の4(5)-メチルイミダゾールのマンセル分析とそのhyperexcitability発症の簡易予見への活用", "subitem_title_language": "ja"}]}, "item_type_id": "4", "owner": "13", "path": ["462"], "permalink_uri": "http://hdl.handle.net/10076/2944", "pubdate": {"attribute_name": "PubDate", "attribute_value": "2007-04-16"}, "publish_date": "2007-04-16", "publish_status": "0", "recid": "5831", "relation": {}, "relation_version_is_last": true, "title": ["アンモニア処理草中の4(5)-メチルイミダゾールのマンセル分析とそのhyperexcitability発症の簡易予見への活用"], "weko_shared_id": -1}
アンモニア処理草中の4(5)-メチルイミダゾールのマンセル分析とそのhyperexcitability発症の簡易予見への活用
http://hdl.handle.net/10076/2944
http://hdl.handle.net/10076/294492b7db13-d88c-4626-b320-4c84bd65e476
名前 / ファイル | ライセンス | アクション |
---|---|---|
AN100738460001902.pdf (383.9 kB)
|
|
Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
---|---|---|---|---|---|---|
公開日 | 2007-04-16 | |||||
タイトル | ||||||
言語 | ja | |||||
タイトル | アンモニア処理草中の4(5)-メチルイミダゾールのマンセル分析とそのhyperexcitability発症の簡易予見への活用 | |||||
言語 | ||||||
言語 | jpn | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | ammonia treatment | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | cereal straw | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | diazo coupling colors | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | hay | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | 4(5)-methylimidazole analysis | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | departmental bulletin paper | |||||
著者 |
横江, 泰彦
× 横江, 泰彦× 後藤, 正和× 西川, 司朗× 萬田, 富治 |
|||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | The contents of 4(5)-methylimidazole (4-MI) in hay and cereal straw treated with different levels of ammonia were investigated by combining ion-pair extraction with reversed-phase ion-pair liquid chromatography (HPLC) and together with photometry of the Ehrich diazo coupling products (λ= 498 nm). The diazo coupling colors corresponding to 4-MI contents in treated roughage were verified and subjected to a panel test, in order to develop a simple procedure for semi-quantitative determination capable to be used on farms. Ammonia-treated hay (3% NH3DM⁻¹) contained 14-81μg g⁻¹DM of 4-MI and the values were increased by increasing the levels of ammonia. 4-MI was not detected in ammonia-treated rice and wheat straw, irrespective of the ammonia levels. A significant correlation between the visible absorbance of 4-MI and HPLC values was found for the ammonia-treated ones. The diazo coupling colors at different4-MI contents were assigned as follows, according to the standard Munsell color table (4-MI ; 0μg g⁻¹DM=5Y8/14 ; 30μg g-1DM=5YR 7/14 ; 50μg g⁻¹DM=5YR 6.5/13 ; 80μg g⁻¹DM=2.5YR 6.5/12 ; 100μg g⁻¹DM=5.5/12 ; 150μg g⁻¹DM=9R 5.5/14 ; 200μg g⁻¹DM=6R 5.5/14). The panel test showed that the 4-MI contents in the ammonia-treated hay were estimated by four groups of None, 30-50, 80-100 and > 100μg g⁻¹DM, according to the Munsell analysis. |
|||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | アンモニア処理された粗飼料中に副生される4(5)-メチルイミダゾール量を,材料の種類(牧草 イネ藁,麦稈)やアンモニア濃度(0,1,2,3,4,6,9%)との関係を検討した。また,生産現場などで簡単に4(5)-メチルイミダゾール量を検出する方法として,ジアゾカップリング呈色皮応によるマンセル値と標準色彩表(色相・明度・彩度)が有効であるかどうかを,パネルテストで判定した。 稲わらや麦稈からの4(5)-メチルイミダゾールは,アンモニア処理の濃度と関係なく,ほとんど検出されなかった。一方,牧乾草の場合には,アンモニア濃度3%処理区で14~81μgg⁻¹DM,6%処理区100~176μgg⁻¹DM,9%処理区127~190μgg⁻¹DMと,アンモニア濃度の増加に対応して4(5)-メチルイミダゾール生成量が増加した。 マンセル値と標準色彩表に基づいたパネルテストによる4(5)-メチルイミダゾールの濃度判定結果は,その濃度が0μggDM⁻¹(ブランク),50μgg⁻¹DM,176μgg⁻¹DMにおいてそれぞれ100%,87.5%,96.0%ときわめて高かった。18.8%の正解率となった30μgg⁻¹DMサンプルはおもに50μgg⁻¹DMと,31.3%の正解率となった100μgg⁻¹DMサンプルは80μgg⁻¹DMと判定された。総じて,パネリストによる判定は正確なものであった。 |
|||||
書誌情報 |
三重大学生物資源学部紀要 = The bulletin of the Faculty of Bioresources, Mie University 巻 19, p. 7-12, 発行日 1997-12-01 |
|||||
ISSN | ||||||
収録物識別子タイプ | PISSN | |||||
収録物識別子 | 0915-0471 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AN10073846 | |||||
フォーマット | ||||||
内容記述タイプ | Other | |||||
内容記述 | application/pdf | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
日本十進分類法 | ||||||
主題Scheme | NDC | |||||
主題 | 643 | |||||
その他のタイトル | ||||||
en | ||||||
Munsell color Analysis of 4(5)-Methylimidazole Produced in Ammonia-treated Forage Relation to a Simple Prediction of Hyperexcitability in Cattle fed These Types of Forage | ||||||
出版者 | ||||||
出版者 | 三重大学生物資源学部 | |||||
ノート | ||||||
Agropedia提供データ | ||||||
資源タイプ(三重大) | ||||||
Departmental Bulletin Paper / 紀要論文 |