{"created":"2023-06-19T11:36:04.702468+00:00","id":2912,"links":{},"metadata":{"_buckets":{"deposit":"26402c92-a0e1-4ab4-ba1a-74b0d1623d9a"},"_deposit":{"created_by":13,"id":"2912","owners":[13],"pid":{"revision_id":0,"type":"depid","value":"2912"},"status":"published"},"_oai":{"id":"oai:mie-u.repo.nii.ac.jp:00002912","sets":["143:144:234:241"]},"author_link":["37405","37406"],"item_4_biblio_info_6":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1984-02-01","bibliographicIssueDateType":"Issued"},"bibliographicPageEnd":"138","bibliographicPageStart":"133","bibliographicVolumeNumber":"35","bibliographic_titles":[{"bibliographic_title":"三重大学教育学部研究紀要. 自然科学"}]}]},"item_4_description_14":{"attribute_name":"フォーマット","attribute_value_mlt":[{"subitem_description":"application/pdf","subitem_description_type":"Other"}]},"item_4_description_4":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A simultaneous determination method for diphenyl(DP)and ortho-phenylphenol(OPP)in citrus fruits, by high performance liquid chromatography(HPLC), was examined. Control and imported fruits were used. For two hrs twice DP and OPP were extracted, by reflux distillation with water, into cyclohexane. HPLC analysis was carried out with Finepak SIL <special>C18-T</special> as packing materials, dilute methanol as mobile phase, and ultraviolet detector at 254nm. The quantitative exactitude of HPLC was confirmed by comparing chromatograms of control fruits with those of contaminated ones. The recovery rates, after adding two preservatives from the control fruits by this method, were 96.7-101.8% for DP after 2 hrs' distillation and 90.5-102.5% for OPP after 4 hrs' distillation. This method has the advantages of simple extraction procedure, lesser solvent consumption, and adequate accuracy. The minimum concentration for determination by this method is 0.1μg DP or OPP per g sample.","subitem_description_type":"Abstract"}]},"item_4_publisher_30":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"三重大学教育学部"}]},"item_4_source_id_7":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"0389-9225","subitem_source_identifier_type":"PISSN"}]},"item_4_source_id_9":{"attribute_name":"書誌レコードID","attribute_value_mlt":[{"subitem_source_identifier":"AN00234199","subitem_source_identifier_type":"NCID"}]},"item_4_text_18":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_text_language":"ja","subitem_text_value":"高速液体クロマトグラフィーによる柑橘類中のジフェニール及びオルトフェニルフェノールの定量"}]},"item_4_text_65":{"attribute_name":"資源タイプ（三重大）","attribute_value_mlt":[{"subitem_text_value":"Departmental Bulletin Paper / 紀要論文"}]},"item_access_right":{"attribute_name":"アクセス権","attribute_value_mlt":[{"subitem_access_right":"metadata only access","subitem_access_right_uri":"http://purl.org/coar/access_right/c_14cb"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"大川, 博徳","creatorNameLang":"ja"},{"creatorName":"Ohkawa, Hironori","creatorNameLang":"en"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"大川, 勝徳","creatorNameLang":"ja"},{"creatorName":"Ohkawa, Masanori","creatorNameLang":"en"}],"nameIdentifiers":[{}]}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"departmental bulletin paper","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"The Determination of Diphenyl and ortho-Phenylphenol in Citrus Fruits by High Performance Liquid Chromatography","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"The Determination of Diphenyl and ortho-Phenylphenol in Citrus Fruits by High Performance Liquid Chromatography","subitem_title_language":"en"}]},"item_type_id":"4","owner":"13","path":["241"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2018-03-16"},"publish_date":"2018-03-16","publish_status":"0","recid":"2912","relation_version_is_last":true,"title":["The Determination of Diphenyl and ortho-Phenylphenol in Citrus Fruits by High Performance Liquid Chromatography"],"weko_creator_id":"13","weko_shared_id":-1},"updated":"2023-11-07T01:50:08.948469+00:00"}