{"created":"2023-06-19T11:36:11.841749+00:00","id":3064,"links":{},"metadata":{"_buckets":{"deposit":"6b1d4dab-dae9-4a68-b717-91087638c0cd"},"_deposit":{"created_by":13,"id":"3064","owners":[13],"pid":{"revision_id":0,"type":"depid","value":"3064"},"status":"published"},"_oai":{"id":"oai:mie-u.repo.nii.ac.jp:00003064","sets":["143:144:234:251"]},"author_link":["37737"],"item_4_biblio_info_6":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1994-03-10","bibliographicIssueDateType":"Issued"},"bibliographicPageEnd":"169","bibliographicPageStart":"159","bibliographicVolumeNumber":"45","bibliographic_titles":[{"bibliographic_title":"三重大学教育学部研究紀要. 自然科学"}]}]},"item_4_description_14":{"attribute_name":"フォーマット","attribute_value_mlt":[{"subitem_description":"application/pdf","subitem_description_type":"Other"}]},"item_4_description_4":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"柑きつ類中の防かび剤ジフェニル及びオルトフェニルフェノールをホモジナイザーで、無水リン酸水素二ナトリウム及び無水硫酸ナトリウムを加えて酢酸エチルで抽出し、蛍光検出器を用いて高速液体クロマトグラフィーで同時定量する方法を確立した。検量線、回収試験及び分析値などから、本法は精度の高い定量分析法であることが証明された。本法を用いて、通年の市販輸入柑きつ類中の両防かび剤の残留量を分析した結果、ジフェニルは全く使用されていないこと、またオルトフェニルフェノールは春から夏にかけて僅かに使われていることがわかった。@@@A simultaneous determination of residual Diphenyl (DP) and ortho-Phenylphenol (OPP) in citrus fruits by High Performance Liquid Chromatography has been established. DP and OPP were extracted with ethyl acetate in the presence of sodium phosphate, dibasic and sodium sulfate by homogenizer and analysed with fluorescence detector. The accuracy of this method was verified by the calibration curves, the recovery rates of DP and OPP added to control citrus fruits and the coefficients of variation of analytical values. The residual DP and OPP in imported citrus fruits were determined throughout the year by this method: DP was not all used whereas OPP was slightly used in spring to summer time.","subitem_description_type":"Abstract"}]},"item_4_publisher_30":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"三重大学教育学部"}]},"item_4_source_id_7":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"0389-9225","subitem_source_identifier_type":"PISSN"}]},"item_4_source_id_9":{"attribute_name":"書誌レコードID","attribute_value_mlt":[{"subitem_source_identifier":"AN00234199","subitem_source_identifier_type":"NCID"}]},"item_4_text_18":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_text_language":"en","subitem_text_value":"The Simultaneous Determination of Residual DP and OPP in Citrus Fruits by HPLC"}]},"item_4_text_65":{"attribute_name":"資源タイプ（三重大）","attribute_value_mlt":[{"subitem_text_value":"Departmental Bulletin Paper / 紀要論文"}]},"item_access_right":{"attribute_name":"アクセス権","attribute_value_mlt":[{"subitem_access_right":"metadata only access","subitem_access_right_uri":"http://purl.org/coar/access_right/c_14cb"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"大川, 博徳","creatorNameLang":"ja"},{"creatorName":"Ohkawa, Hironori","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"37737","nameIdentifierScheme":"WEKO"}]}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"departmental bulletin paper","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"高速液体クロマトグラフィーによる柑きつ類中の残存DP及びOPPの同時定量法","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"高速液体クロマトグラフィーによる柑きつ類中の残存DP及びOPPの同時定量法","subitem_title_language":"ja"}]},"item_type_id":"4","owner":"13","path":["251"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2018-03-16"},"publish_date":"2018-03-16","publish_status":"0","recid":"3064","relation_version_is_last":true,"title":["高速液体クロマトグラフィーによる柑きつ類中の残存DP及びOPPの同時定量法"],"weko_creator_id":"13","weko_shared_id":-1},"updated":"2023-11-07T05:09:07.210831+00:00"}